Proline derived guanidine catalysts forge extensive H-bonded architectures: a solution and solid state study
Authors of publication
Al-Taie, Zahraa S.; Anetts, Simon R.; Christensen, Jeppe; Coles, Simon J.; Horton, Peter N.; Evans, Daniel M.; Jones, Leigh F.; de Kleijne, Frank F. J.; Ledbetter, Shaun M.; Mehdar, Yassin T. H.; Murphy, Patrick J.; Wilson, Jack A.
Journal of publication
RSC Advances
Year of publication
2020
Journal volume
10
Journal issue
38
Pages of publication
22397 - 22416
a
8.2749 ± 0.0001 Å
b
9.8955 ± 0.0001 Å
c
21.8743 ± 0.0003 Å
α
82.107 ± 0.001°
β
86.694 ± 0.001°
γ
85.775 ± 0.001°
Cell volume
1767.32 ± 0.04 Å3
Cell temperature
30 ± 2 K
Ambient diffraction temperature
30 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0866
Residual factor for significantly intense reflections
0.0817
Weighted residual factors for significantly intense reflections
0.226
Weighted residual factors for all reflections included in the refinement
0.2295
Goodness-of-fit parameter for all reflections included in the refinement
