Crystallography Open Database

Information card for entry 7242713

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Coordinates	7242713.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H28 N16 Na4 O12 W2
Calculated formula	C32 H28 N16 Na4 O12 W2
Title of publication	Unusual structural changes going from Li+ to Cs+ in [W(CN)6(bpy)]2− ion salts: the Na+ case
Authors of publication	Hodorowicz, Maciej; Jurowska, Anna; Szklarzewicz, Janusz
Journal of publication	CrystEngComm
Year of publication	2021
Journal volume	23
Journal issue	24
Pages of publication	4301 - 4311
a	12.1359 ± 0.0003 Å
b	13.8894 ± 0.0003 Å
c	13.9395 ± 0.0003 Å
α	92.898 ± 0.002°
β	97.773 ± 0.002°
γ	100.49 ± 0.002°
Cell volume	2282.32 ± 0.09 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	129.9 ± 0.6 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0575
Residual factor for significantly intense reflections	0.0349
Weighted residual factors for significantly intense reflections	0.0629
Weighted residual factors for all reflections included in the refinement	0.0711
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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