Information card for entry 7242714

Structure parameters

• Formula: C18 H11 N9 Na2 O4.9 W
• Calculated formula: C18 H11 N9 Na2 O4.872 W
• Title of publication: Unusual structural changes going from Li+ to Cs+ in [W(CN)6(bpy)]2− ion salts: the Na+ case
• Authors of publication: Hodorowicz, Maciej; Jurowska, Anna; Szklarzewicz, Janusz
• Journal of publication: CrystEngComm
• Year of publication: 2021
• Journal volume: 23
• Journal issue: 24
• Pages of publication: 4301 - 4311
• a: 8.5595 ± 0.0002 Å
• b: 9.8622 ± 0.0001 Å
• c: 13.8861 ± 0.0003 Å
• α: 94.349 ± 0.001°
• β: 99.66 ± 0.002°
• γ: 98.206 ± 0.001°
• Cell volume: 1137.75 ± 0.04 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0542
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.1191
• Weighted residual factors for all reflections included in the refinement: 0.1232
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No