Information card for entry 7700133

Structure parameters

• Formula: C78 H82 O16 Pd4
• Calculated formula: C78 H82 O16 Pd4
• Title of publication: Chiral tectonics toward square planar tetranuclear Pd(ii) complexes: propagation of axial chirality through a long molecular axis.
• Authors of publication: Goto, Yutaro; Watanabe, Yutaka; Noboriguchi, Aoki; Yoshida, Jun; Mori, Shigeki; Sato, Hisako
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 27
• Pages of publication: 10138 - 10144
• a: 13.9277 ± 0.0003 Å
• b: 14.837 ± 0.0003 Å
• c: 19.9949 ± 0.0004 Å
• α: 104.707 ± 0.002°
• β: 100.001 ± 0.002°
• γ: 108.914 ± 0.002°
• Cell volume: 3629.76 ± 0.16 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0829
• Residual factor for significantly intense reflections: 0.0499
• Weighted residual factors for significantly intense reflections: 0.0923
• Weighted residual factors for all reflections included in the refinement: 0.1026
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No