Information card for entry 7700134

Structure parameters

• Formula: C40 H36 Cl4 O8 Pd2
• Calculated formula: C40 H36 Cl4 O8 Pd2
• Title of publication: Chiral tectonics toward square planar tetranuclear Pd(ii) complexes: propagation of axial chirality through a long molecular axis.
• Authors of publication: Goto, Yutaro; Watanabe, Yutaka; Noboriguchi, Aoki; Yoshida, Jun; Mori, Shigeki; Sato, Hisako
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 27
• Pages of publication: 10138 - 10144
• a: 21.4114 ± 0.0006 Å
• b: 16.1953 ± 0.0004 Å
• c: 11.4025 ± 0.0002 Å
• α: 90°
• β: 94.113 ± 0.002°
• γ: 90°
• Cell volume: 3943.79 ± 0.16 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0638
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for significantly intense reflections: 0.083
• Weighted residual factors for all reflections included in the refinement: 0.09
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No