Information card for entry 7700687

Structure parameters

• Formula: C24 H37 B2 F8 N5 Ni
• Calculated formula: C24 H37 B2 F8 N5 Ni
• Title of publication: Cu(i), Ag(i), Ni(ii), Cr(iii) and Ir(i) complexes with tritopic N^imineC^NHCN^amine pincer ligands and catalytic ethylene oligomerization.
• Authors of publication: Ren, Xiaoyu; Wesolek, Marcel; Braunstein, Pierre
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 34
• Pages of publication: 12895 - 12909
• a: 12.6898 ± 0.0004 Å
• b: 12.7224 ± 0.0004 Å
• c: 20.949 ± 0.0006 Å
• α: 90°
• β: 119.931 ± 0.002°
• γ: 90°
• Cell volume: 2931.02 ± 0.17 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0739
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for significantly intense reflections: 0.1014
• Weighted residual factors for all reflections included in the refinement: 0.1154
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No