Information card for entry 7700686

Structure parameters

• Formula: C44 H68 Cu4 I4 N8
• Calculated formula: C44 H68 Cu4 I4 N8
• Title of publication: Cu(i), Ag(i), Ni(ii), Cr(iii) and Ir(i) complexes with tritopic N^imineC^NHCN^amine pincer ligands and catalytic ethylene oligomerization.
• Authors of publication: Ren, Xiaoyu; Wesolek, Marcel; Braunstein, Pierre
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 34
• Pages of publication: 12895 - 12909
• a: 15.7098 ± 0.0008 Å
• b: 8.6227 ± 0.0002 Å
• c: 22.1783 ± 0.001 Å
• α: 90°
• β: 119.744 ± 0.003°
• γ: 90°
• Cell volume: 2608.5 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.102
• Residual factor for significantly intense reflections: 0.0555
• Weighted residual factors for significantly intense reflections: 0.1164
• Weighted residual factors for all reflections included in the refinement: 0.1559
• Goodness-of-fit parameter for all reflections included in the refinement: 1.096
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No