Information card for entry 7700691

Structure parameters

• Formula: C30 H46 Cl Ir N4
• Calculated formula: C30 H46 Cl Ir N4
• Title of publication: Cu(i), Ag(i), Ni(ii), Cr(iii) and Ir(i) complexes with tritopic N^imineC^NHCN^amine pincer ligands and catalytic ethylene oligomerization.
• Authors of publication: Ren, Xiaoyu; Wesolek, Marcel; Braunstein, Pierre
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 34
• Pages of publication: 12895 - 12909
• a: 8.4032 ± 0.0004 Å
• b: 11.1493 ± 0.0005 Å
• c: 16.7862 ± 0.0007 Å
• α: 105.21 ± 0.001°
• β: 104.489 ± 0.001°
• γ: 96.004 ± 0.001°
• Cell volume: 1444.74 ± 0.11 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0254
• Residual factor for significantly intense reflections: 0.0199
• Weighted residual factors for significantly intense reflections: 0.0424
• Weighted residual factors for all reflections included in the refinement: 0.0441
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No