Information card for entry 7700693

Structure parameters

• Formula: C25 H42 Ge N2 P2
• Calculated formula: C25 H42 Ge N2 P2
• Title of publication: A dipyrromethane-based diphosphane-germylene as precursor to tetrahedral copper(i) and T-shaped silver(i) and gold(i) PGeP pincer complexes.
• Authors of publication: Cabeza, Javier A.; Fernández, Israel; García-Álvarez, Pablo; Laglera-Gándara, Carlos J
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 35
• Pages of publication: 13273 - 13280
• a: 11.4095 ± 0.0006 Å
• b: 17.4206 ± 0.0007 Å
• c: 14.326 ± 0.0006 Å
• α: 90°
• β: 112.581 ± 0.006°
• γ: 90°
• Cell volume: 2629.1 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0661
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for significantly intense reflections: 0.1163
• Weighted residual factors for all reflections included in the refinement: 0.129
• Goodness-of-fit parameter for all reflections included in the refinement: 1.139
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No