Information card for entry 7700694

Structure parameters

• Formula: C43 H57 Cl Cu Ge N2 P3
• Calculated formula: C43 H57 Cl Cu Ge N2 P3
• Title of publication: A dipyrromethane-based diphosphane-germylene as precursor to tetrahedral copper(i) and T-shaped silver(i) and gold(i) PGeP pincer complexes.
• Authors of publication: Cabeza, Javier A.; Fernández, Israel; García-Álvarez, Pablo; Laglera-Gándara, Carlos J
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 35
• Pages of publication: 13273 - 13280
• a: 15.9072 ± 0.0002 Å
• b: 13.5272 ± 0.0002 Å
• c: 19.6745 ± 0.0002 Å
• α: 90°
• β: 92.328 ± 0.001°
• γ: 90°
• Cell volume: 4230.06 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0336
• Residual factor for significantly intense reflections: 0.0281
• Weighted residual factors for significantly intense reflections: 0.0689
• Weighted residual factors for all reflections included in the refinement: 0.0721
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No