Information card for entry 7700715
| Formula |
C32 H48 B2 N8 Ni |
| Calculated formula |
C32 H48 B2 N8 Ni |
| Title of publication |
Synthesis and characterization of bis(pyrazolyl)borate Ni(ii) complexes: ligand rearrangement and transformation. |
| Authors of publication |
Zhao, Qianyi; Guan, Xin-Ting; Dou, Ting; Cao, Hou-Ji; Ma, Na-Na; Xu, Ting; Gao, Peng-Hui; Kong, Xiao-Hua; Zhang, Jie; Chen, Xuenian |
| Journal of publication |
Dalton transactions (Cambridge, England : 2003) |
| Year of publication |
2019 |
| Journal volume |
48 |
| Journal issue |
35 |
| Pages of publication |
13242 - 13247 |
| a |
7.5038 ± 0.0005 Å |
| b |
9.7847 ± 0.0005 Å |
| c |
11.3835 ± 0.0006 Å |
| α |
87.799 ± 0.004° |
| β |
79.365 ± 0.005° |
| γ |
68.035 ± 0.006° |
| Cell volume |
761.39 ± 0.08 Å3 |
| Cell temperature |
295.2 ± 0.4 K |
| Ambient diffraction temperature |
295.2 ± 0.4 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0542 |
| Residual factor for significantly intense reflections |
0.0464 |
| Weighted residual factors for significantly intense reflections |
0.1178 |
| Weighted residual factors for all reflections included in the refinement |
0.1239 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.03 |
| Diffraction radiation probe |
x-ray |
| Diffraction radiation wavelength |
1.54184 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/7700715.html
