Information card for entry 7700715

Structure parameters

• Formula: C32 H48 B2 N8 Ni
• Calculated formula: C32 H48 B2 N8 Ni
• Title of publication: Synthesis and characterization of bis(pyrazolyl)borate Ni(ii) complexes: ligand rearrangement and transformation.
• Authors of publication: Zhao, Qianyi; Guan, Xin-Ting; Dou, Ting; Cao, Hou-Ji; Ma, Na-Na; Xu, Ting; Gao, Peng-Hui; Kong, Xiao-Hua; Zhang, Jie; Chen, Xuenian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 35
• Pages of publication: 13242 - 13247
• a: 7.5038 ± 0.0005 Å
• b: 9.7847 ± 0.0005 Å
• c: 11.3835 ± 0.0006 Å
• α: 87.799 ± 0.004°
• β: 79.365 ± 0.005°
• γ: 68.035 ± 0.006°
• Cell volume: 761.39 ± 0.08 ų
• Cell temperature: 295.2 ± 0.4 K
• Ambient diffraction temperature: 295.2 ± 0.4 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0542
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.1178
• Weighted residual factors for all reflections included in the refinement: 0.1239
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No