Information card for entry 7700784

Structure parameters

• Formula: C31 H18 B F9 N2
• Calculated formula: C31 H18 B F9 N2
• Title of publication: Reactions of hydrazones and hydrazides with Lewis acidic boranes.
• Authors of publication: Gazis, Theodore A.; Dasgupta, Ayan; Hill, Michael S.; Rawson, Jeremy M.; Wirth, Thomas; Melen, Rebecca L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 33
• Pages of publication: 12391 - 12395
• a: 9.5166 ± 0.0004 Å
• b: 21.8157 ± 0.0008 Å
• c: 13.1104 ± 0.0005 Å
• α: 90°
• β: 99.132 ± 0.004°
• γ: 90°
• Cell volume: 2687.37 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0531
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.0965
• Weighted residual factors for all reflections included in the refinement: 0.1045
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No