Information card for entry 7700783

Structure parameters

• Formula: C58 H34 B2 Cl4 F18 N4
• Calculated formula: C58 H34 B2 Cl4 F18 N4
• Title of publication: Reactions of hydrazones and hydrazides with Lewis acidic boranes.
• Authors of publication: Gazis, Theodore A.; Dasgupta, Ayan; Hill, Michael S.; Rawson, Jeremy M.; Wirth, Thomas; Melen, Rebecca L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 33
• Pages of publication: 12391 - 12395
• a: 9.4053 ± 0.0006 Å
• b: 11.2224 ± 0.0007 Å
• c: 13.6936 ± 0.0008 Å
• α: 103.791 ± 0.005°
• β: 98.886 ± 0.005°
• γ: 90.099 ± 0.005°
• Cell volume: 1385.73 ± 0.15 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1335
• Residual factor for significantly intense reflections: 0.0645
• Weighted residual factors for significantly intense reflections: 0.1206
• Weighted residual factors for all reflections included in the refinement: 0.1608
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No