Crystallography Open Database

Information card for entry 7700940

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Coordinates	7700940.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H46 Cl O P Pd
Calculated formula	C39 H46 Cl O P Pd
Title of publication	Palladium-mediated intramolecular dearomatization of ligated dialkylterphenyl phosphines.
Authors of publication	Rama, Raquel J.; Maya, Celia; Nicasio, M. Carmen
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	39
Pages of publication	14575 - 14579
a	11.8653 ± 0.0005 Å
b	12.3384 ± 0.0005 Å
c	12.5433 ± 0.0005 Å
α	82.432 ± 0.002°
β	75.828 ± 0.002°
γ	69.56 ± 0.002°
Cell volume	1666.18 ± 0.12 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.052
Residual factor for significantly intense reflections	0.0364
Weighted residual factors for significantly intense reflections	0.0801
Weighted residual factors for all reflections included in the refinement	0.093
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	0.56086 Å
Diffraction radiation type	AgKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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