Information card for entry 7700941

Structure parameters

• Formula: C34 H40 Cl P Pd
• Calculated formula: C34 H40 Cl P Pd
• Title of publication: Palladium-mediated intramolecular dearomatization of ligated dialkylterphenyl phosphines.
• Authors of publication: Rama, Raquel J.; Maya, Celia; Nicasio, M. Carmen
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 39
• Pages of publication: 14575 - 14579
• a: 15.8449 ± 0.0006 Å
• b: 13.447 ± 0.0006 Å
• c: 15.8973 ± 0.0006 Å
• α: 90°
• β: 118.137 ± 0.0014°
• γ: 90°
• Cell volume: 2986.9 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0497
• Residual factor for significantly intense reflections: 0.0346
• Weighted residual factors for significantly intense reflections: 0.0858
• Weighted residual factors for all reflections included in the refinement: 0.0933
• Goodness-of-fit parameter for all reflections included in the refinement: 0.901
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No