Information card for entry 7700997

Structure parameters

• Formula: C16 H64 Ge Mo2 N4 O47 W10
• Calculated formula: C16 H48 Ge Mo1.966 N4 O43 W10.034
• Title of publication: A "directed precursor self-assembly" strategy for the facile synthesis of heteropoly blues: crystal structures, formation mechanism and electron distribution.
• Authors of publication: Wang, Yuchao; Li, Fengyan; Jiang, Ning; Liu, Xizheng; Xu, Lin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 38
• Pages of publication: 14347 - 14353
• a: 13.1465 ± 0.0012 Å
• b: 20.8579 ± 0.0019 Å
• c: 22.4 ± 0.002 Å
• α: 90°
• β: 92.772 ± 0.001°
• γ: 90°
• Cell volume: 6135.1 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.078
• Residual factor for significantly intense reflections: 0.0476
• Weighted residual factors for significantly intense reflections: 0.1112
• Weighted residual factors for all reflections included in the refinement: 0.1251
• Goodness-of-fit parameter for all reflections included in the refinement: 0.995
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No