Information card for entry 7701499

Structure parameters

• Formula: C32 H80 Si12
• Calculated formula: C32 H80 Si12
• Title of publication: Reactions of a tetrasilabicyclo[1.1.0]but-1(3)-ene with carbon tetrachloride and methanol.
• Authors of publication: Nukazawa, Takumi; Kosai, Tomoyuki; Honda, Shunya; Ishida, Shintaro; Iwamoto, Takeaki
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 29
• Pages of publication: 10874 - 10880
• a: 9.2308 ± 0.0005 Å
• b: 11.5172 ± 0.0006 Å
• c: 13.2387 ± 0.0006 Å
• α: 64.958 ± 0.001°
• β: 75.308 ± 0.001°
• γ: 66.788 ± 0.001°
• Cell volume: 1165.54 ± 0.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0485
• Residual factor for significantly intense reflections: 0.0333
• Weighted residual factors for significantly intense reflections: 0.0787
• Weighted residual factors for all reflections included in the refinement: 0.0832
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No