Information card for entry 7701500

Structure parameters

• Formula: C36 H91 Cl2 O Si12
• Calculated formula: C36 H91 Cl2 O Si12
• Title of publication: Reactions of a tetrasilabicyclo[1.1.0]but-1(3)-ene with carbon tetrachloride and methanol.
• Authors of publication: Nukazawa, Takumi; Kosai, Tomoyuki; Honda, Shunya; Ishida, Shintaro; Iwamoto, Takeaki
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 29
• Pages of publication: 10874 - 10880
• a: 18.4326 ± 0.0008 Å
• b: 12.7398 ± 0.0006 Å
• c: 23.2524 ± 0.001 Å
• α: 90°
• β: 93.1569 ± 0.0012°
• γ: 90°
• Cell volume: 5452 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0504
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.1065
• Weighted residual factors for all reflections included in the refinement: 0.113
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No