Information card for entry 7701537

Structure parameters

• Formula: C135 H132 B4 F42 N4
• Calculated formula: C135 H132 B4 F42 N4
• Title of publication: Isolation of base stabilized fluoroborylene and its radical cation.
• Authors of publication: Sarkar, Samir Kumar; Siddiqui, Mujahuddin M.; Kundu, Subrata; Ghosh, Munmun; Kretsch, Johannes; Stollberg, Peter; Herbst-Irmer, Regine; Stalke, Dietmar; Stückl, A Claudia; Schwederski, Brigitte; Kaim, Wolfgang; Ghorai, Sagar; Jemmis, Eluvathingal D.; Roesky, Herbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 24
• Pages of publication: 8551 - 8555
• a: 27.121 ± 0.004 Å
• b: 28.125 ± 0.004 Å
• c: 21.074 ± 0.003 Å
• α: 90°
• β: 128.85 ± 0.02°
• γ: 90°
• Cell volume: 12519 ± 5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0967
• Residual factor for significantly intense reflections: 0.0729
• Weighted residual factors for significantly intense reflections: 0.1444
• Weighted residual factors for all reflections included in the refinement: 0.1538
• Goodness-of-fit parameter for all reflections included in the refinement: 1.223
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No