Information card for entry 7701553

Structure parameters

• Formula: C22 H62 K2 N4 O2 Si4
• Calculated formula: C22 H62 K2 N4 O2 Si4
• Title of publication: Bis(trimethylsilyl)amide complexes of s-block metals with bidentate ether and amine ligands.
• Authors of publication: Schüler, Philipp; Görls, Helmar; Westerhausen, Matthias; Krieck, Sven
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 24
• Pages of publication: 8966 - 8975
• a: 9.7712 ± 0.0003 Å
• b: 10.493 ± 0.0004 Å
• c: 11.019 ± 0.0004 Å
• α: 70.532 ± 0.002°
• β: 65.43 ± 0.002°
• γ: 73.177 ± 0.002°
• Cell volume: 953.62 ± 0.06 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0478
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.0849
• Weighted residual factors for all reflections included in the refinement: 0.0901
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No