Crystallography Open Database

Information card for entry 7701554

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Coordinates	7701554.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H62 Ba N4 O2 Si4
Calculated formula	C22 H62 Ba N4 O2 Si4
Title of publication	Bis(trimethylsilyl)amide complexes of s-block metals with bidentate ether and amine ligands.
Authors of publication	Schüler, Philipp; Görls, Helmar; Westerhausen, Matthias; Krieck, Sven
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	24
Pages of publication	8966 - 8975
a	23.5555 ± 0.0004 Å
b	10.2892 ± 0.0002 Å
c	17.2253 ± 0.0003 Å
α	90°
β	118.317 ± 0.001°
γ	90°
Cell volume	3675.27 ± 0.12 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0171
Residual factor for significantly intense reflections	0.0163
Weighted residual factors for significantly intense reflections	0.0394
Weighted residual factors for all reflections included in the refinement	0.0398
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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