Information card for entry 7701645

Structure parameters

• Formula: C30 H49 B P2
• Calculated formula: C30 H49 B P2
• Title of publication: Structural and spectroscopic analysis of a new family of monomeric diphosphinoboranes.
• Authors of publication: Ordyszewska, Anna; Szynkiewicz, Natalia; Perzanowski, Emil; Chojnacki, Jarosław; Wiśniewska, Aleksandra; Grubba, Rafał
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 33
• Pages of publication: 12482 - 12495
• a: 26.974 ± 0.0015 Å
• b: 6.4025 ± 0.0003 Å
• c: 33.146 ± 0.0015 Å
• α: 90°
• β: 90.429 ± 0.004°
• γ: 90°
• Cell volume: 5724.2 ± 0.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.0623
• Residual factor for significantly intense reflections: 0.0477
• Weighted residual factors for significantly intense reflections: 0.1231
• Weighted residual factors for all reflections included in the refinement: 0.1307
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No