Information card for entry 7701646

Structure parameters

• Formula: C14 H32 B Br N P
• Calculated formula: C14 H32 B Br N P
• Title of publication: Structural and spectroscopic analysis of a new family of monomeric diphosphinoboranes.
• Authors of publication: Ordyszewska, Anna; Szynkiewicz, Natalia; Perzanowski, Emil; Chojnacki, Jarosław; Wiśniewska, Aleksandra; Grubba, Rafał
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 33
• Pages of publication: 12482 - 12495
• a: 8.14383 ± 0.00018 Å
• b: 14.2729 ± 0.0004 Å
• c: 15.9925 ± 0.0004 Å
• α: 90°
• β: 100.262 ± 0.0017°
• γ: 90°
• Cell volume: 1829.17 ± 0.08 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0474
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.0738
• Weighted residual factors for all reflections included in the refinement: 0.0803
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No