Tetranuclear grid-like copper(II) complexes with pyrazolate bridges: syntheses, structures, magnetic and EPR spectroscopic properties
Authors of publication
Mann, Karen L. V.; Psillakis, Elefteria; Jeffery, John C.; Rees, Leigh H.; Harden, Nicholas M.; McCleverty, Jon A.; Ward, Michael D.; Gatteschi, Dante; Totti, Federico; Mabbs,, Frank E.; McInnes, Eric J. L.; Riedi, Peter C.; Smith, Graham M.
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
1999
Journal issue
3
Pages of publication
339
a
11.5877 ± 0.0014 Å
b
12.651 ± 0.002 Å
c
21.63 ± 0.004 Å
α
90°
β
96.208 ± 0.013°
γ
90°
Cell volume
3152.3 ± 0.9 Å3
Cell temperature
171 ± 2 K
Ambient diffraction temperature
171 ± 2 K
Number of distinct elements
7
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0735
Residual factor for significantly intense reflections
0.0603
Weighted residual factors for all reflections
0.1699
Weighted residual factors for significantly intense reflections
0.1549
Goodness-of-fit parameter for all reflections
1.068
Goodness-of-fit parameter for significantly intense reflections
