Tetranuclear grid-like copper(II) complexes with pyrazolate bridges: syntheses, structures, magnetic and EPR spectroscopic properties
Authors of publication
Mann, Karen L. V.; Psillakis, Elefteria; Jeffery, John C.; Rees, Leigh H.; Harden, Nicholas M.; McCleverty, Jon A.; Ward, Michael D.; Gatteschi, Dante; Totti, Federico; Mabbs,, Frank E.; McInnes, Eric J. L.; Riedi, Peter C.; Smith, Graham M.
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
1999
Journal issue
3
Pages of publication
339
a
10.41 ± 0.002 Å
b
13.282 ± 0.003 Å
c
14.17 ± 0.002 Å
α
85.254 ± 0.01°
β
70.087 ± 0.012°
γ
68.15 ± 0.02°
Cell volume
1707.6 ± 0.6 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0392
Residual factor for significantly intense reflections
0.036
Weighted residual factors for all reflections
0.1056
Weighted residual factors for significantly intense reflections
0.0989
Goodness-of-fit parameter for all reflections
0.934
Goodness-of-fit parameter for significantly intense reflections
