Information card for entry 7702389

Structure parameters

• Formula: C24 H54 Cl2 Co2 N10 O4 S2
• Calculated formula: C24 H54 Cl2 Co2 N10 O8 S2
• Title of publication: Preparation of the first sulfur-containing cobalt and nickel complexes stabilised by the macrocyclic cyclam ligand; observation of S‒H bond activation
• Authors of publication: Pleus, Rainer J.; Waden, Harald; Saak, Wolfgang; Haase, Detlev; Pohl, Siegfried
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 15
• Pages of publication: 2601
• a: 12.899 ± 0.003 Å
• b: 13.879 ± 0.003 Å
• c: 21.201 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3795.5 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 22
• Hermann-Mauguin space group symbol: F 2 2 2
• Hall space group symbol: F 2 2
• Residual factor for all reflections: 0.088
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for all reflections: 0.1736
• Weighted residual factors for significantly intense reflections: 0.1331
• Goodness-of-fit parameter for all reflections: 1.213
• Goodness-of-fit parameter for significantly intense reflections: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No