Crystallography Open Database

Information card for entry 7702390

Preview

Coordinates	7702390.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C61 H136 I10 N5 O1.5 Pb3
Calculated formula	C61 H136 I10 N5 O1.5 Pb3
Title of publication	Discrete and polymeric iodoplumbates with Pb3I10 building blocks: [Pb3I10]4−, [Pb7I22]8−, [Pb10I28]8−, 1\ιnfty [Pb3I10]4− and 2∞[Pb7I18]4−
Authors of publication	Krautscheid, Harald; Vielsack, Frieder
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	16
Pages of publication	2731
a	15.3391 ± 0.0009 Å
b	16.9204 ± 0.001 Å
c	20.6738 ± 0.0014 Å
α	72.963 ± 0.005°
β	70.719 ± 0.005°
γ	74.467 ± 0.004°
Cell volume	4754.8 ± 0.5 Å³
Cell temperature	210 ± 2 K
Ambient diffraction temperature	210 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0723
Residual factor for significantly intense reflections	0.0474
Weighted residual factors for significantly intense reflections	0.1071
Weighted residual factors for all reflections included in the refinement	0.1246
Goodness-of-fit parameter for all reflections included in the refinement	1.096
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKa
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7702390.html