Information card for entry 7702391

Structure parameters

• Formula: C112 H248 I22 N8 Pb7
• Calculated formula: C109.6 H241.6 I22 N8 Pb7
• Title of publication: Discrete and polymeric iodoplumbates with Pb3I10 building blocks: [Pb3I10]4−, [Pb7I22]8−, [Pb10I28]8−, 1\ιnfty [Pb3I10]4− and 2∞[Pb7I18]4−
• Authors of publication: Krautscheid, Harald; Vielsack, Frieder
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 16
• Pages of publication: 2731
• a: 16.73 ± 0.002 Å
• b: 26.823 ± 0.003 Å
• c: 20.496 ± 0.002 Å
• α: 90°
• β: 105.87 ± 0.01°
• γ: 90°
• Cell volume: 8847 ± 1.7 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0597
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for significantly intense reflections: 0.0961
• Weighted residual factors for all reflections included in the refinement: 0.1022
• Goodness-of-fit parameter for all reflections included in the refinement: 0.924
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No