Information card for entry 7702428

Structure parameters

• Formula: C22 H53 Li N6 Si3
• Calculated formula: C22 H55 Li N6 Si3
• Title of publication: Reactions of 1,3,5-triazine with organolithium compounds containing trimethylsilyl substituents; X-ray structures of 1,3,5-triaza- and 1,3,5,7-tetraaza-heptatrienyllithium compounds †
• Authors of publication: Boesveld, W. Marco; Hitchcock, Peter B.; Lappert, Michael F.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 22
• Pages of publication: 4041
• a: 28.389 ± 0.005 Å
• b: 11.343 ± 0.002 Å
• c: 10.29 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3313.5 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.1059
• Residual factor for significantly intense reflections: 0.0605
• Weighted residual factors for all reflections: 0.1575
• Weighted residual factors for significantly intense reflections: 0.1362
• Goodness-of-fit parameter for all reflections: 1.025
• Goodness-of-fit parameter for significantly intense reflections: 1.122
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No