Information card for entry 7702429

Structure parameters

• Formula: C40 H88 Li4 N12 Si8
• Calculated formula: C40 H88 Li4 N12 Si8
• Title of publication: Reactions of 1,3,5-triazine with organolithium compounds containing trimethylsilyl substituents; X-ray structures of 1,3,5-triaza- and 1,3,5,7-tetraaza-heptatrienyllithium compounds †
• Authors of publication: Boesveld, W. Marco; Hitchcock, Peter B.; Lappert, Michael F.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 22
• Pages of publication: 4041
• a: 10.047 ± 0.003 Å
• b: 12.148 ± 0.004 Å
• c: 13.646 ± 0.003 Å
• α: 82.42 ± 0.02°
• β: 76.68 ± 0.02°
• γ: 76.74 ± 0.02°
• Cell volume: 1572 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0769
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for all reflections: 0.1242
• Weighted residual factors for significantly intense reflections: 0.1088
• Goodness-of-fit parameter for all reflections: 1.03
• Goodness-of-fit parameter for significantly intense reflections: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No