Information card for entry 7702717

Structure parameters

• Formula: C8 H24 Cl2 N3 O9 Rh S3
• Calculated formula: C8 H22 Cl2 N3 O9 Rh S3
• Title of publication: Rhodium(iii) complexes with thiolate and thioether ligands derived from fac(S)-[Rh(aet)3] (aet = 2-aminoethanethiolate): selective formation, characterization and properties
• Authors of publication: Hirotsu, Masakazu; Kobayashi, Atsushi; Yoshimura, Takashi; Konno, Takumi
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 878
• a: 9.368 ± 0.002 Å
• b: 16.306 ± 0.002 Å
• c: 13.167 ± 0.001 Å
• α: 90°
• β: 96.413 ± 0.01°
• γ: 90°
• Cell volume: 1998.7 ± 0.5 ų
• Cell temperature: 293.2 K
• Ambient diffraction temperature: 293.2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0262
• Weighted residual factors for significantly intense reflections: 0.0248
• Goodness-of-fit parameter for significantly intense reflections: 2.574
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No