Information card for entry 7702718

Structure parameters

• Formula: C18 H58 Cl6 N6 O26 Rh2 S6
• Calculated formula: C18 H54 Cl6 N6 O26 Rh2 S6
• Title of publication: Rhodium(iii) complexes with thiolate and thioether ligands derived from fac(S)-[Rh(aet)3] (aet = 2-aminoethanethiolate): selective formation, characterization and properties
• Authors of publication: Hirotsu, Masakazu; Kobayashi, Atsushi; Yoshimura, Takashi; Konno, Takumi
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 878
• a: 19.181 ± 0.004 Å
• b: 14.374 ± 0.004 Å
• c: 20.233 ± 0.004 Å
• α: 90°
• β: 116.93 ± 0.01°
• γ: 90°
• Cell volume: 4973 ± 2 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.0487
• Weighted residual factors for significantly intense reflections: 0.0347
• Goodness-of-fit parameter for significantly intense reflections: 1.572
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No