Information card for entry 7702918

Structure parameters

• Formula: C140 H161 Gd6 N13 Na2 O70
• Calculated formula: C138 H127 Gd6 N13 Na2 O55
• Title of publication: Synthesis, structures and magnetic properties of a family of nitrate-bridged octanuclear [Na2Ln6] (Ln = Dy, Tb, Gd, Sm) complexes.
• Authors of publication: She, Shixiong; Chen, Yanmei; Zaworotko, Michael J.; Liu, Wei; Cao, Yanyuan; Wu, Jian; Li, Yahong
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 29
• Pages of publication: 10433 - 10438
• a: 28.6753 ± 0.0015 Å
• b: 19.3572 ± 0.001 Å
• c: 30.6841 ± 0.0016 Å
• α: 90°
• β: 104.296 ± 0.003°
• γ: 90°
• Cell volume: 16504.5 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0695
• Residual factor for significantly intense reflections: 0.0511
• Weighted residual factors for significantly intense reflections: 0.1532
• Weighted residual factors for all reflections included in the refinement: 0.1663
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No