Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7702935
Preview
Coordinates | 7702935.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C15 H25 Cl2 O P Ru |
---|---|
Calculated formula | C15 H25 Cl2 O P Ru |
Title of publication | Half-sandwich ruthenium(ii) complexes with tethered arene-phosphinite ligands: synthesis, structure and application in catalytic cross dehydrogenative coupling reactions of silanes and alcohols. |
Authors of publication | González-Fernández, Rebeca; Crochet, Pascale; Cadierno, Victorio |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2020 |
Journal volume | 49 |
Journal issue | 1 |
Pages of publication | 210 - 222 |
a | 8.9634 ± 0.0002 Å |
b | 13.7539 ± 0.0003 Å |
c | 27.5 ± 0.0006 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3390.25 ± 0.13 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0324 |
Residual factor for significantly intense reflections | 0.0302 |
Weighted residual factors for significantly intense reflections | 0.0892 |
Weighted residual factors for all reflections included in the refinement | 0.0918 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.118 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7702935.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.