Information card for entry 7702969

Structure parameters

• Formula: C49 H58 Ge O2 P2 Si
• Calculated formula: C45 H48 Ge O P2 Si
• Title of publication: Avenue to phosphaalkenes from Ph₃GePCO.
• Authors of publication: Szkop, Kevin M.; Jupp, Andrew R.; Razumkov, Hlib; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 3
• Pages of publication: 885 - 890
• a: 12.244 ± 0.009 Å
• b: 13.196 ± 0.009 Å
• c: 16.49 ± 0.012 Å
• α: 109.25 ± 0.03°
• β: 93.811 ± 0.019°
• γ: 105.368 ± 0.013°
• Cell volume: 2391 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1211
• Residual factor for significantly intense reflections: 0.0555
• Weighted residual factors for significantly intense reflections: 0.1058
• Weighted residual factors for all reflections included in the refinement: 0.1201
• Goodness-of-fit parameter for all reflections included in the refinement: 0.937
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No