Information card for entry 7702970

Structure parameters

• Formula: C45 H48 Ge O P2 Si
• Calculated formula: C45 H48 Ge O P2 Si
• Title of publication: Avenue to phosphaalkenes from Ph₃GePCO.
• Authors of publication: Szkop, Kevin M.; Jupp, Andrew R.; Razumkov, Hlib; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 3
• Pages of publication: 885 - 890
• a: 16.0049 ± 0.0015 Å
• b: 16.34 ± 0.002 Å
• c: 18.646 ± 0.002 Å
• α: 113.791 ± 0.003°
• β: 94.049 ± 0.003°
• γ: 110.342 ± 0.003°
• Cell volume: 4055.4 ± 0.8 ų
• Cell temperature: 149 ± 2 K
• Ambient diffraction temperature: 149.53 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0931
• Residual factor for significantly intense reflections: 0.0417
• Weighted residual factors for significantly intense reflections: 0.0892
• Weighted residual factors for all reflections included in the refinement: 0.1067
• Goodness-of-fit parameter for all reflections included in the refinement: 0.988
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No