Information card for entry 7703007

Structure parameters

• Formula: C12 H60 Ge2 Mo20 N24 Ni7 O90
• Calculated formula: C12 H60 Ge2 Mo20 N24 Ni7 O90
• Title of publication: Two Ni/Co-substituted sandwich-type germanomolybdates based on an unprecedented trivacant polyanion [α-GeMo₁₀O₃₆]⁸.
• Authors of publication: Xu, Hui; Liu, Xing-Man; Su, Tan; Chen, Wei-Chao; Su, Zhong-Min
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 4
• Pages of publication: 977 - 982
• a: 13.933 ± 0.0019 Å
• b: 14.2147 ± 0.0019 Å
• c: 14.591 ± 0.002 Å
• α: 110.716 ± 0.002°
• β: 98.574 ± 0.002°
• γ: 112.773 ± 0.002°
• Cell volume: 2351.2 ± 0.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0483
• Residual factor for significantly intense reflections: 0.0351
• Weighted residual factors for significantly intense reflections: 0.0824
• Weighted residual factors for all reflections included in the refinement: 0.0893
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No