Information card for entry 7703008

Structure parameters

• Formula: C12 H62 Co7 Ge2 Mo20 N24 O91
• Calculated formula: C12 H62 Co7 Ge2 Mo20 N24 O91
• Title of publication: Two Ni/Co-substituted sandwich-type germanomolybdates based on an unprecedented trivacant polyanion [α-GeMo₁₀O₃₆]⁸.
• Authors of publication: Xu, Hui; Liu, Xing-Man; Su, Tan; Chen, Wei-Chao; Su, Zhong-Min
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 4
• Pages of publication: 977 - 982
• a: 13.9114 ± 0.0012 Å
• b: 14.1874 ± 0.0012 Å
• c: 14.6356 ± 0.0013 Å
• α: 110.55 ± 0.004°
• β: 98.559 ± 0.004°
• γ: 112.651 ± 0.004°
• Cell volume: 2357.5 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0405
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for significantly intense reflections: 0.0675
• Weighted residual factors for all reflections included in the refinement: 0.0716
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No