Information card for entry 7703266

Structure parameters

• Formula: C34 H15 B Cl0.4 F20.6 Sb
• Calculated formula: C34 H15 B Cl0.4 F20.6 Sb
• Title of publication: Diverse structure and reactivity of pentamethylcyclopentadienyl antimony(iii) cations.
• Authors of publication: Coughlin, Omar; Krämer, Tobias; Benjamin, Sophie L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 6
• Pages of publication: 1726 - 1730
• a: 10.6582 ± 0.0003 Å
• b: 12.6174 ± 0.0004 Å
• c: 12.8229 ± 0.0003 Å
• α: 90.784 ± 0.002°
• β: 95.717 ± 0.002°
• γ: 105.278 ± 0.003°
• Cell volume: 1653.76 ± 0.08 ų
• Cell temperature: 150.01 ± 0.1 K
• Ambient diffraction temperature: 150.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1352
• Residual factor for significantly intense reflections: 0.0813
• Weighted residual factors for significantly intense reflections: 0.1308
• Weighted residual factors for all reflections included in the refinement: 0.1464
• Goodness-of-fit parameter for all reflections included in the refinement: 1.158
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No