Information card for entry 7703267

Structure parameters

• Formula: C58 H41 B F22 N2 Sb
• Calculated formula: C58 H41 B F22 N2 Sb
• Title of publication: Diverse structure and reactivity of pentamethylcyclopentadienyl antimony(iii) cations.
• Authors of publication: Coughlin, Omar; Krämer, Tobias; Benjamin, Sophie L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 6
• Pages of publication: 1726 - 1730
• a: 18.2924 ± 0.0002 Å
• b: 17.8036 ± 0.0002 Å
• c: 17.4223 ± 0.0002 Å
• α: 90°
• β: 113.529 ± 0.001°
• γ: 90°
• Cell volume: 5202.19 ± 0.11 ų
• Cell temperature: 150.01 ± 0.1 K
• Ambient diffraction temperature: 150.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0884
• Residual factor for significantly intense reflections: 0.0823
• Weighted residual factors for significantly intense reflections: 0.2431
• Weighted residual factors for all reflections included in the refinement: 0.2467
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No