Information card for entry 7703685

Structure parameters

• Formula: C71 H69 B F24 N O2 P2 Rh
• Calculated formula: C71 H69 B F24 N O2 P2 Rh
• Title of publication: Synthesis and rhodium complexes of macrocyclic PNP and PONOP pincer ligands.
• Authors of publication: Hood, Thomas M.; Gyton, Matthew R.; Chaplin, Adrian B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 7
• Pages of publication: 2077 - 2086
• a: 13.44737 ± 0.0001 Å
• b: 13.57276 ± 0.0001 Å
• c: 38.9533 ± 0.0003 Å
• α: 90°
• β: 94.8285 ± 0.0007°
• γ: 90°
• Cell volume: 7084.44 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0792
• Residual factor for significantly intense reflections: 0.0768
• Weighted residual factors for significantly intense reflections: 0.1977
• Weighted residual factors for all reflections included in the refinement: 0.1994
• Goodness-of-fit parameter for all reflections included in the refinement: 1.11
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No