Information card for entry 7703686

Structure parameters

• Formula: C60.5 H62 B Cl F24 N O3 P2 Rh
• Calculated formula: C60.5 H62 B Cl F24 N O3 P2 Rh
• Title of publication: Synthesis and rhodium complexes of macrocyclic PNP and PONOP pincer ligands.
• Authors of publication: Hood, Thomas M.; Gyton, Matthew R.; Chaplin, Adrian B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 7
• Pages of publication: 2077 - 2086
• a: 26.48866 ± 0.00018 Å
• b: 18.27115 ± 0.00017 Å
• c: 27.8172 ± 0.0002 Å
• α: 90°
• β: 93.5082 ± 0.0006°
• γ: 90°
• Cell volume: 13437.7 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0862
• Residual factor for significantly intense reflections: 0.0719
• Weighted residual factors for significantly intense reflections: 0.1919
• Weighted residual factors for all reflections included in the refinement: 0.2087
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No