Crystallography Open Database

Information card for entry 7703687

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Coordinates	7703687.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C73 H73 B F24 N P2 Rh
Calculated formula	C73 H73 B F24 N P2 Rh
Title of publication	Synthesis and rhodium complexes of macrocyclic PNP and PONOP pincer ligands.
Authors of publication	Hood, Thomas M.; Gyton, Matthew R.; Chaplin, Adrian B.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	7
Pages of publication	2077 - 2086
a	13.6274 ± 0.00016 Å
b	13.36471 ± 0.00014 Å
c	39.2179 ± 0.0005 Å
α	90°
β	95.3071 ± 0.001°
γ	90°
Cell volume	7111.99 ± 0.14 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0421
Residual factor for significantly intense reflections	0.036
Weighted residual factors for significantly intense reflections	0.0864
Weighted residual factors for all reflections included in the refinement	0.0901
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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