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Information card for entry 7703687
Preview
Coordinates | 7703687.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C73 H73 B F24 N P2 Rh |
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Calculated formula | C73 H73 B F24 N P2 Rh |
Title of publication | Synthesis and rhodium complexes of macrocyclic PNP and PONOP pincer ligands. |
Authors of publication | Hood, Thomas M.; Gyton, Matthew R.; Chaplin, Adrian B. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2020 |
Journal volume | 49 |
Journal issue | 7 |
Pages of publication | 2077 - 2086 |
a | 13.6274 ± 0.00016 Å |
b | 13.36471 ± 0.00014 Å |
c | 39.2179 ± 0.0005 Å |
α | 90° |
β | 95.3071 ± 0.001° |
γ | 90° |
Cell volume | 7111.99 ± 0.14 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0421 |
Residual factor for significantly intense reflections | 0.036 |
Weighted residual factors for significantly intense reflections | 0.0864 |
Weighted residual factors for all reflections included in the refinement | 0.0901 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7703687.html
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Users of the data should acknowledge the original authors of the
structural data.