Information card for entry 7703862

Structure parameters

• Formula: C39 H53 Cl2 N O3 Si2 W
• Calculated formula: C39 H53 Cl2 N O3 Si2 W
• Title of publication: Synthesis, structure, and reactivity of a pyridine-stabilized silanonetungsten complex.
• Authors of publication: Muraoka, Takako; Tsuchimoto, Masato; Ueno, Keiji
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 16
• Pages of publication: 5100 - 5107
• a: 14.969 ± 0.005 Å
• b: 16.001 ± 0.005 Å
• c: 19.069 ± 0.006 Å
• α: 91.88 ± 0.005°
• β: 109.446 ± 0.006°
• γ: 110.618 ± 0.005°
• Cell volume: 3972 ± 2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0401
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.0903
• Weighted residual factors for all reflections included in the refinement: 0.0925
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No