Information card for entry 7703927

Structure parameters

• Chemical name: Cu4(PN)4 THF
• Formula: C240 H548 Cu16 N64 O4 P16
• Calculated formula: C240 H548 Cu16 N64 O4 P16
• Title of publication: Coinage metal tris(dialkylamido)imidophosphorane complexes as transmetallation reagents for cerium complexes.
• Authors of publication: Aguirre Quintana, Luis M.; Jiang, Ningxin; Bacsa, John; La Pierre, Henry S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 17
• Pages of publication: 5420 - 5423
• a: 13.463 ± 0.002 Å
• b: 22.899 ± 0.004 Å
• c: 24.461 ± 0.004 Å
• α: 90°
• β: 93.561 ± 0.007°
• γ: 90°
• Cell volume: 7527 ± 2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 99.99 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0791
• Residual factor for significantly intense reflections: 0.0451
• Weighted residual factors for significantly intense reflections: 0.0953
• Weighted residual factors for all reflections included in the refinement: 0.1123
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No