Information card for entry 7704123

Structure parameters

• Formula: C38 H45 F24 N4 Nd O11
• Calculated formula: C38 H45 F24 N4 Nd O11
• Title of publication: Synthesis, structural characterization and electrochemical and magnetic studies of M(hfac)₂ (M = Cu^II, Co^II) and Nd(hfac)₃ complexes of 4-amino-TEMPO.
• Authors of publication: Navarro, Yolanda; Guedes, Guilherme P.; Cano, Joan; Ocón, Pilar; Iglesias, María José; Lloret, Francisco; López-Ortiz, Fernando
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 19
• Pages of publication: 6280 - 6294
• a: 16.6805 ± 0.0005 Å
• b: 11.8287 ± 0.0004 Å
• c: 27.8879 ± 0.0011 Å
• α: 90°
• β: 105.118 ± 0.002°
• γ: 90°
• Cell volume: 5312.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0572
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1155
• Weighted residual factors for all reflections included in the refinement: 0.1213
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No