Synthesis, structural characterization and electrochemical and magnetic studies of M(hfac)<sub>2</sub> (M = Cu<sup>II</sup>, Co<sup>II</sup>) and Nd(hfac)<sub>3</sub> complexes of 4-amino-TEMPO.
Authors of publication
Navarro, Yolanda; Guedes, Guilherme P.; Cano, Joan; Ocón, Pilar; Iglesias, María José; Lloret, Francisco; López-Ortiz, Fernando
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2020
Journal volume
49
Journal issue
19
Pages of publication
6280 - 6294
a
11.5195 ± 0.0003 Å
b
19.0369 ± 0.0005 Å
c
19.033 ± 0.0006 Å
α
90°
β
90.392 ± 0.002°
γ
90°
Cell volume
4173.8 ± 0.2 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.074
Residual factor for significantly intense reflections
0.0616
Weighted residual factors for significantly intense reflections
0.1287
Weighted residual factors for all reflections included in the refinement
0.1355
Goodness-of-fit parameter for all reflections included in the refinement
