Information card for entry 7704221

Structure parameters

• Chemical name: [Ce(Htp)2(BH4)2K(THF)(Et2O)]n
• Formula: C32 H66 B2 Ce K O2 P2
• Calculated formula: C32 H66 B2 Ce K O2 P2
• Title of publication: Synthesis and characterisation of light lanthanide bis-phospholyl borohydride complexes.
• Authors of publication: Liu, Jingjing; Nodaraki, Lydia E.; Cobb, Philip J.; Giansiracusa, Marcus J.; Ortu, Fabrizio; Tuna, Floriana; Mills, David P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 19
• Pages of publication: 6504 - 6511
• a: 19.861 ± 0.001 Å
• b: 15.8524 ± 0.0006 Å
• c: 12.8759 ± 0.0007 Å
• α: 90°
• β: 106.613 ± 0.006°
• γ: 90°
• Cell volume: 3884.7 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0821
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.0767
• Weighted residual factors for all reflections included in the refinement: 0.087
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No