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Information card for entry 7704310
Preview
Coordinates | 7704310.cif |
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Original paper (by DOI) | HTML |
Formula | C50 H80.06 Br0.94 Ge N2 O4.06 S2 Si4 |
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Calculated formula | C50 H80.06 Br0.94 Ge N2 O4.06 S2 Si4 |
Title of publication | 1,2-Insertion reactions of alkynes into Ge-C bonds of arylbromogermylene. |
Authors of publication | Sugahara, Tomohiro; Espinosa Ferao, Arturo; Rey Planells, Alicia; Guo, Jing-Dong; Aoyama, Shin; Igawa, Kazunobu; Tomooka, Katsuhiko; Sasamori, Takahiro; Hashizume, Daisuke; Nagase, Shigeru; Tokitoh, Norihiro |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2020 |
Journal volume | 49 |
Journal issue | 21 |
Pages of publication | 7189 - 7196 |
a | 10.7385 ± 0.0001 Å |
b | 20.7088 ± 0.0002 Å |
c | 26.3913 ± 0.0003 Å |
α | 76.872 ± 0.001° |
β | 88.089 ± 0.001° |
γ | 78.773 ± 0.001° |
Cell volume | 5605.81 ± 0.1 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0598 |
Residual factor for significantly intense reflections | 0.0381 |
Weighted residual factors for significantly intense reflections | 0.0819 |
Weighted residual factors for all reflections included in the refinement | 0.0893 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.018 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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