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Information card for entry 7704311
Preview
Coordinates | 7704311.cif |
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Original paper (by DOI) | HTML |
Formula | C48 H76 Br Ge N2 O4 S2 Si4 |
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Calculated formula | C48 H76 Br Ge N2 O4 S2 Si4 |
Title of publication | 1,2-Insertion reactions of alkynes into Ge-C bonds of arylbromogermylene. |
Authors of publication | Sugahara, Tomohiro; Espinosa Ferao, Arturo; Rey Planells, Alicia; Guo, Jing-Dong; Aoyama, Shin; Igawa, Kazunobu; Tomooka, Katsuhiko; Sasamori, Takahiro; Hashizume, Daisuke; Nagase, Shigeru; Tokitoh, Norihiro |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2020 |
Journal volume | 49 |
Journal issue | 21 |
Pages of publication | 7189 - 7196 |
a | 10.5431 ± 0.0002 Å |
b | 20.8098 ± 0.0003 Å |
c | 26.3903 ± 0.0004 Å |
α | 76.58 ± 0.001° |
β | 88.846 ± 0.001° |
γ | 77.458 ± 0.001° |
Cell volume | 5494.74 ± 0.16 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0932 |
Residual factor for significantly intense reflections | 0.0558 |
Weighted residual factors for significantly intense reflections | 0.1198 |
Weighted residual factors for all reflections included in the refinement | 0.1344 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7704311.html
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